TY - EJOU
AU - Yasinova, S. N.
AU - Rzayeva, A. B.
AU - Huseynaliyev, M. H.
AU - Hagieva, B. T.
AU - Huseynov, G. M.
TI - Thermogravimetric analysis of the PbS, PbSe and PbS0.5Se0.5 powders obtained by chemical precipitation
T2 - Chalcogenide Letters
PY - 2025
VL - 22
IS - 10
SN - 1584-8663
AB - The thin films and powders of PbS, PbSe, and PbSe and PbS0.5Se0.5 have been obtained by chemical
precipitation method. The X-ray spectra of the obtained thin layers were obtained through
the"Miniflex 600" diffractometer, and elemental analyses were performed.
Thermogravimetric analyses of the powders of all three compounds were conducted in the
temperature range of 20-800°C using the "NETZSCH STA 449 F3" apparatus. It has been
determined from the X-ray spectra that the angular positions of all the peaks of PbS, PbSe,
and PbSe and PbS0.5Se0.5 thin layers coincide with the positions of the corresponding diffraction
peaks obtained under normal conditions. The results of the thermogravimetric analysis
measurements and calculations have shown that the compounds are consistent with the
formulas of PbS, PbSe, and PbS0.5Se0.5 powders.
KW - Thin film
KW - Chemical bath
KW - X-Ray
KW - Thermogravimetric analysis (TGA)
KW - Lead chalcogenides
DO - 10.15251/CL.2025.2210.883