@Article{JPM.2019.36.04.8,
AUTHOR = {JALPA V. CHOPDA, DHARMESH B. SANKHAVARA, JIGNESH P. PATEL, P. H. PARSANIA},
TITLE = {Synthesis and Characterization of Epoxy methacrylate of (2E, 6E)-Bis(4-hydroxybenzylidene)-4- methylcyclohexanone},
JOURNAL = {Journal of Polymer Materials},
VOLUME = {36},
YEAR = {2019},
NUMBER = {4},
PAGES = {391--399},
URL = {http://www.techscience.com/jpm/v36n4/56093},
ISSN = {0976-3449},
ABSTRACT = {The epoxymethcrylate resin (EMBHBCMA) of (2E, 6E)-bis(4-hydroxybenzylidene)-4-
methylcyclohexanone(EMBHBC) was synthesized by condensing EMBHBC and methacrylic
acid (1:2 mole ratio) by using 1,4-dioxane as a solvent and triethylamine as a catalyst at reflux
temperature for 1-5 h to get acid value < 10. The structure of EMBHBCMA was supported by
UV-Vis, FTIR, <sup>1</sup>
HNMR and <sup>13</sup>CNMR spectroscopic techniques. Molecular weights and molecular
weight distribution of EMBHBCMA were determined by gel permeation chromatography.
EMBHBCMA is thermally stable up to about 300°C and followed two step degradation reactions.
Kinetic parameters such as n, Ea, A and ΔS* were determined according to Anderson-Freeman
method and discussed.},
DOI = {10.32381/JPM.2019.36.04.8}
}