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    ARTICLE

    Ultrasound-Assisted Synthesis of Sucrose and Fructooligosaccharides Esters as Bio-Plasticizers

    Dragomir Vassilev1*, Nadezhda Petkova2, Milena Koleva1, Panteley Denev2

    Journal of Renewable Materials, Vol.4, No.1, pp. 24-30, 2016, DOI:10.7569/JRM.2015.634125

    Abstract This article presents the results obtained by the ultrasound-assisted synthesis of sucrose and fructooligosaccharides (FOS) esters with fatty acids (palmitic and 10-undecylenic), the identifi cation of the products and the study of their possible application as plasticizers in plastics processing. Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (1H and 13C NMR) spectroscopy were used to identify the synthesized carbohydrate esters. The plasticizing effect of the sucrose palmitate applied in polyvinyl chloride (PVC) was evaluated by the glass transition temperatures; the decrease of the Tg with the increase of the ester content could be accepted as confi rmation of… More >

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