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ARTICLE
Synthesis and Characterization of Epoxy Resin of (2E, 6E) - Bis (4-hydroxybenzylidene) -4-methylcyclohexanone
JALPA V. CHOPDA, DHARMESH B. SANKHAVARA, JIGNESH P. PATEL, P. H. PARSANIA*
Department of Chemistry, Saurashtra University, Rajkot-360 005, Gujarat, India
* Corresponding Authors: e-mail: and
Journal of Polymer Materials 2019, 36(1), 101-109. https://doi.org/10.32381/JPM.2019.36.01.8
Abstract
The epoxy resin (EMBHBC) of (2E,6E)-bis (4-hydroxybenzylidene)-4-methyl cyclohexanone
(MBHBC) was synthesized by condensing 0.5 mol MBHBC and 2.5 mol epichlorohydrin in 500
mL isopropyl alcohol as a solvent and 1.0 mol NaOH in 50 mL water as a catalyst at 80°C for 3 h.
The structure of EMBHBC was supported by UV-Vis, FTIR,
1
HNMR and
13CNMR spectroscopic
techniques. Molecular weights and molecular weight distribution of EMBHBC were determined
by gel permeation chromatography. DSC thermogram of EMBHC showed one endothermic
transition (95.9°C) and two exothermic transitions (317.7°C and 382.2°C) due to melting and
decomposition transitions, respectively. EMBHBC is thermally stable up to about 293°C and
followed two step degradation reactions.
Keywords
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APA Style
CHOPDA, J.V., SANKHAVARA, D.B., PATEL, J.P., PARSANIA, P.H. (2019). Synthesis and characterization of epoxy resin of (2E, 6E) - bis (4-hydroxybenzylidene) -4-methylcyclohexanone. Journal of Polymer Materials, 36(1), 101-109. https://doi.org/10.32381/JPM.2019.36.01.8
Vancouver Style
CHOPDA JV, SANKHAVARA DB, PATEL JP, PARSANIA PH. Synthesis and characterization of epoxy resin of (2E, 6E) - bis (4-hydroxybenzylidene) -4-methylcyclohexanone. J Polym Materials . 2019;36(1):101-109 https://doi.org/10.32381/JPM.2019.36.01.8
IEEE Style
J.V. CHOPDA, D.B. SANKHAVARA, J.P. PATEL, and P.H. PARSANIA "Synthesis and Characterization of Epoxy Resin of (2E, 6E) - Bis (4-hydroxybenzylidene) -4-methylcyclohexanone," J. Polym. Materials , vol. 36, no. 1, pp. 101-109. 2019. https://doi.org/10.32381/JPM.2019.36.01.8