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ARTICLE
Synthesis and Characterization of Epoxy methacrylate of (2E, 6E)-Bis(4-hydroxybenzylidene)-4- methylcyclohexanone
JALPA V. CHOPDA, DHARMESH B. SANKHAVARA, JIGNESH P. PATEL, P. H. PARSANIA*
Department of Chemistry, Saurashtra University, Rajkot-360 005, Gujarat, India
* Corresponding Authors: e-mail:,
Journal of Polymer Materials 2019, 36(4), 391-399. https://doi.org/10.32381/JPM.2019.36.04.8
Abstract
The epoxymethcrylate resin (EMBHBCMA) of (2E, 6E)-bis(4-hydroxybenzylidene)-4-
methylcyclohexanone(EMBHBC) was synthesized by condensing EMBHBC and methacrylic
acid (1:2 mole ratio) by using 1,4-dioxane as a solvent and triethylamine as a catalyst at reflux
temperature for 1-5 h to get acid value < 10. The structure of EMBHBCMA was supported by
UV-Vis, FTIR,
1
HNMR and
13CNMR spectroscopic techniques. Molecular weights and molecular
weight distribution of EMBHBCMA were determined by gel permeation chromatography.
EMBHBCMA is thermally stable up to about 300°C and followed two step degradation reactions.
Kinetic parameters such as n, Ea, A and ΔS* were determined according to Anderson-Freeman
method and discussed.
Keywords
Cite This Article
APA Style
CHOPDA, J.V., SANKHAVARA, D.B., PATEL, J.P., PARSANIA, P.H. (2019). Synthesis and characterization of epoxy methacrylate of (2E, 6e)-bis(4-hydroxybenzylidene)-4- methylcyclohexanone. Journal of Polymer Materials, 36(4), 391-399. https://doi.org/10.32381/JPM.2019.36.04.8
Vancouver Style
CHOPDA JV, SANKHAVARA DB, PATEL JP, PARSANIA PH. Synthesis and characterization of epoxy methacrylate of (2E, 6e)-bis(4-hydroxybenzylidene)-4- methylcyclohexanone. J Polym Materials . 2019;36(4):391-399 https://doi.org/10.32381/JPM.2019.36.04.8
IEEE Style
J.V. CHOPDA, D.B. SANKHAVARA, J.P. PATEL, and P.H. PARSANIA "Synthesis and Characterization of Epoxy methacrylate of (2E, 6E)-Bis(4-hydroxybenzylidene)-4- methylcyclohexanone," J. Polym. Materials , vol. 36, no. 4, pp. 391-399. 2019. https://doi.org/10.32381/JPM.2019.36.04.8