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    ARTICLE

    Carrageenan Fiber Prepared by a New Process Route of Ba2+ Ion Pre-Crosslinking in the Spinning Solution

    Liting Jia1, Xiao Han1, Cuixia Qiao2, Gang Zhao2, Yanzhi Xia1, Zhixin Xue1,*

    Journal of Renewable Materials, Vol.12, No.3, pp. 427-441, 2024, DOI:10.32604/jrm.2023.044310

    Abstract Ba2+ pre-crosslinked carrageenan fiber (Ba/CAF) was prepared by adding a small amount of Ba2+ to the carrageenan (CA) solution as the spinning solution. Ba/CAF-n/A, Ba/CAF-n/B and Ba/CAF-n/C were prepared with ethanol solution (combine A), high concentration BaCl2 solution (combine B) and low concentration BaCl2 solution (combine C), as coagulation bath and stretch bath, respectively. The combination of coagulation bath and stretch bath suitable for Ba2+ pre-crosslinking wet spinning was screened. The results showed that Ba2+ can induce the birefringence of the CA molecular chain, and the Ba2+ pre-crosslinking effect is the best when the CA mass fraction is 8.0 wt%.… More > Graphic Abstract

    Carrageenan Fiber Prepared by a New Process Route of Ba<sup>2+</sup> Ion Pre-Crosslinking in the Spinning Solution

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