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  • Open Access

    ARTICLE

    Synthesis and Physico-Chemical Analysis of Epoxy Methacrylate of (2E, 6E)-2,6-Bis(4- hydroxybenzylidene)cyclohexanone

    DHARMESH B. SANKHAVARA, JALPA V. CHOPDA, JIGNESH P. PATEL, PARSOTAM H. PARSANIA*

    Journal of Polymer Materials, Vol.36, No.4, pp. 371-379, 2019, DOI:10.32381/JPM.2019.36.04.6

    Abstract The epoxy methacrylate of (2E,6E)-2, 6-bis(4-hydroxybenzylidene)cyclohexanone (EBHBCMA) was synthesized by condensing 0.02 equi. EBHBC, 0.04 equi. methacrylic acid, 50 mL THF as a solvent and 0.2 mL triethylamine as a catalyst at reflux temperature for 1-5 h to get acid value < 10. EBHBCMA showed good solubility in common solvents. The structure of EBHBCMA was supported by UV-Vis., FTIR, 1 H NMR, and 13C NMR spectroscopic techniques. DSC thermogram of EBHBCMA exhibited two endothermic peaks (86.4 and 117.1 °C) and one exothermic peak (142.6°C) due to moisture release, melting and curing of the resin, respectively. More >

  • Open Access

    ARTICLE

    Synthesis and Characterization of Epoxy Resin of (2E, 6E) - Bis (4-hydroxybenzylidene) -4-methylcyclohexanone

    JALPA V. CHOPDA, DHARMESH B. SANKHAVARA, JIGNESH P. PATEL, P. H. PARSANIA*

    Journal of Polymer Materials, Vol.36, No.1, pp. 101-109, 2019, DOI:10.32381/JPM.2019.36.01.8

    Abstract The epoxy resin (EMBHBC) of (2E,6E)-bis (4-hydroxybenzylidene)-4-methyl cyclohexanone (MBHBC) was synthesized by condensing 0.5 mol MBHBC and 2.5 mol epichlorohydrin in 500 mL isopropyl alcohol as a solvent and 1.0 mol NaOH in 50 mL water as a catalyst at 80°C for 3 h. The structure of EMBHBC was supported by UV-Vis, FTIR, 1 HNMR and 13CNMR spectroscopic techniques. Molecular weights and molecular weight distribution of EMBHBC were determined by gel permeation chromatography. DSC thermogram of EMBHC showed one endothermic transition (95.9°C) and two exothermic transitions (317.7°C and 382.2°C) due to melting and decomposition transitions, respectively. More >

  • Open Access

    ARTICLE

    Synthesis and Physico-chemical Studies on Chalcone Based Epoxy Resin of (2E, 6E)-Bis (4-hydroxybenzylidene) cyclohexanone

    DHARMESH B. SANKHAVARA, JALPA CHOPDA, JIGNESH P. PATEL, P. H. PARSANIA*

    Journal of Polymer Materials, Vol.36, No.1, pp. 13-21, 2019, DOI:10.32381/JPM.2019.36.01.2

    Abstract Chalcone based epoxy resin (EBHBC) of (2E, 6E)- bis(4-hydroxybenzylidene) cyclohexanone (BHBC) was synthesized by condensing 0.5 mol BHBC and 2.5 mol epichlorohydrin in 500 mL isopropanol as a solvent and 1.0 mol NaOH in 50 mL water as a catalyst at 80o C. The structure of EBHBC is supported by spectral techniques. Molecular weights and molecular weight distribution of EBHBC were determined by gel permeation chromatography. DSC thermogram of EBHC showed one endothermic transition (146.1°C) and two endothermic transitions (253.52°C and 397.34°C) due to melting, some physical change and decomposition transitions, respectively. EBHBC is thermally More >

  • Open Access

    ARTICLE

    Use of vasoactive agents in postoperative pediatric cardiac patients: Insights from a national database

    Rohit S. Loomba1, Saul Flores2

    Congenital Heart Disease, Vol.14, No.6, pp. 1176-1184, 2019, DOI:10.1111/chd.12837

    Abstract Objective: The main goal of this study is to examine the variation in vasoactive agent prescription patterns across a large cohort of patients. In addition, we sought to determine the association between the number of vasoactive agents used during admissions and characteristics of admissions utilizing varying numbers of vasoactive agents.
    Methods: This was a multi-institutional, cross-sectional study of the pediatric health information system database of patients who underwent congenital heart surgery and received vasoactive agents from 2004 to 2015. The international classification of disease-9 (ICD-9) codes were used to select admissions to those only pertaining to cardiac… More >

  • Open Access

    ARTICLE

    High Capacity Data Hiding in Encrypted Image Based on Compressive Sensing for Nonequivalent Resources

    Di Xiao1,*, Jia Liang1, Qingqing Ma1, Yanping Xiang1, Yushu Zhang2

    CMC-Computers, Materials & Continua, Vol.58, No.1, pp. 1-13, 2019, DOI:10.32604/cmc.2019.02171

    Abstract To fulfill the requirements of data security in environments with nonequivalent resources, a high capacity data hiding scheme in encrypted image based on compressive sensing (CS) is proposed by fully utilizing the adaptability of CS to nonequivalent resources. The original image is divided into two parts: one part is encrypted with traditional stream cipher; the other part is turned to the prediction error and then encrypted based on CS to vacate room simultaneously. The collected non-image data is firstly encrypted with simple stream cipher. For data security management, the encrypted non-image data is then embedded More >

  • Open Access

    ARTICLE

    Tanshinone Suppresses Arecoline-Induced Epithelial–Mesenchymal Transition in Oral Submucous Fibrosis by Epigenetically Reactivating the p53 Pathway

    Lian Zheng, Zhen-Jie Guan, Wen-Ting Pan, Tian-Feng Du, Yu-Jia Zhai, Jia Guo

    Oncology Research, Vol.26, No.3, pp. 483-494, 2018, DOI:10.3727/096504017X14941825760362

    Abstract Oral submucous fibrosis (OSF) induced by chewing of the areca nut has been considered to be a precancerous lesion with a high probability of developing oral squamous cell carcinoma. Tanshinone (TSN) is the main component extracted from Salvia miltiorrhiza, a traditional Chinese medicine, which was found to have diverse pharmacological effects, such as anti-inflammatory and antitumor. In the current study, we aimed to identify the inhibitory effects and the underlying mechanism of TSN on OSF progress. We found that treatment with TSN inhibited the arecoline-mediated proliferation of primary human oral mucosal fibroblasts and reversed the… More >

  • Open Access

    RETRACTION

    Retraction Notice to: Mitigating Content Caching Attack in NDN

    Zhiqiang Ruan1,*, Haibo Luo1, Wenzhong Lin1, Jie Wang2

    CMC-Computers, Materials & Continua, Vol.57, No.3, pp. 653-653, 2018, DOI:10.32604/cmc.2018.00653

    Abstract none More >

  • Open Access

    ARTICLE

    Superoxide and hydrogen peroxide productions by NO-inhibited complex III

    Darío E. IGLESIAS*, Silvina S. BOMBICINO, Alberto BOVERIS, Laura B. VALDEZ

    BIOCELL, Vol.40, No.1, pp. 27-30, 2016, DOI:10.32604/biocell.2016.40.027

    Abstract Complex III plays a central role in the mitochondrial respiratory chain transferring electrons from ubiquinol to cytochrome c and pumping protons to the intermembrane space, contributing to the protonmotive force. Furthermore, complex III can act as a source of O2 •- in the presence of ubiquinol and antimycin, an expermiental condition in which the oxidation of the cytochrome b hemes is blocked. The O2 •- dismutation catalyzed by superoxide dismutase produces H2O2, a known second messenger in redox signalling. Results from our laboratory have shown that NO, released from GSNO or from SPER -NO or generated… More >

  • Open Access

    ARTICLE

    Method for Detecting Macroscopic Irregularities in Gears Based on Template Matching and the Nonequivalence Operation

    W.C. Wang1, F.L. Chang2, Y.L. Liu1, X. J. Wu1

    CMES-Computer Modeling in Engineering & Sciences, Vol.107, No.5, pp. 411-431, 2015, DOI:10.3970/cmes.2015.107.411

    Abstract The detection of macroscopic irregularities is an essential procedure during the production of gears, and it helps to guarantee the quality of electromechanical transmission equipment. The working principles of template matching and the image nonequivalence operation are described in detail in this paper. Gray-level transformation, edge-preserving filtering, image segmentation, feature extraction, and pattern recognition were analyzed, leading to the design of a defect detection system based on template matching and the nonequivalence operation, followed by the development of a hardware platform and application software for the system. The experimental results indicate that the proposed detection More >

  • Open Access

    ARTICLE

    Oral administration of hesperidin, a citrus flavonone, in rats counteracts the oxidative stress, the inflammatory cytokine production, and the hepatotoxicity induced by the ingestion of 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)

    Recep Bentli1, Osman Ciftci2, Asli Cetin3, Merve Unlu2, Nese Basak2, Mahmut Çay4

    European Cytokine Network, Vol.24, No.2, pp. 91-96, 2013, DOI:10.1684/ecn.2013.0337

    Abstract The objective of the current study was to investigate the protective effects of hesperidin against oxidative stress, altered cytokines levels and histological changes in rats induced by 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD). Rats were divided randomly into four equal groups (Control, TCDD, hesperidin and TCDD+hesperidin). TCDD and hesperidin were given by gavage, dissolved in corn oil at doses of 2 μ/kg/week and 50 mg/kg/day respectively. The blood and tissue samples were taken from all rats on the 60th day, to be analyzed for the determination of oxidative stress, histological changes and cytokine levels. The results indicated that hesperidin prevented More >

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